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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 19
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Original Articles

The Synthesis of 4-Amino-2-methyl-3-(1-oxo) Pent-4-ynyl-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-b]pyridine

David Bolton SmithKline Beecham Pharmaceuticals, The Pinnacles, Harlow, Essex CM19, 5AD, UK
,
Amanda Johns SmithKline Beecham Pharmaceuticals, The Pinnacles, Harlow, Essex CM19, 5AD, UK
&
Mervyn Thompson SmithKline Beecham Pharmaceuticals, The Pinnacles, Harlow, Essex CM19, 5AD, UK
Pages 2683-2689 | Received 13 May 1993, Published online: 23 Sep 2006
 
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Abstract

The synthesis of ketone 1 from the ethyl ester of 4-amino-2-methyl-5,6,7,8-tetrahydrobenzo[b]thieno[2,3-b]pyridine-3-carboxylic acid using β-ketosulfone methodology is described.

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