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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 1
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Original Articles

A Facile Preparation of N,N-Disilylbenzylamines from Benzylic Chlorides Using AgI/LiN(SiMe3)2 System

Toshiaki Murai Department of Chemistry, Faculty of Engineering, Gifu University, Yanagido, Gifu, 501-11, Japan
,
Masaki Ogami Department of Chemistry, Faculty of Engineering, Gifu University, Yanagido, Gifu, 501-11, Japan
,
Fumio Tsujimura Department of Chemistry, Faculty of Engineering, Gifu University, Yanagido, Gifu, 501-11, Japan
,
Hideharu Ishihara Department of Chemistry, Faculty of Engineering, Gifu University, Yanagido, Gifu, 501-11, Japan
&
Shinzi Kato Department of Chemistry, Faculty of Engineering, Gifu University, Yanagido, Gifu, 501-11, Japan
Pages 7-14 | Accepted 13 Jul 1992, Published online: 24 Sep 2006
 
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Abstract

The reaction of benzylic chlorides with lithium N,N-bis(trimethylsilyl)amide in the presence of AgI gives the corresponding N,N-disilylbenzylamines in good to excellent yields. The amounts of AgI used are highly dependent on the substrates.

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