A Procedure for the Large Scale Preparation of Nε-Alloc-lysine and Nε-Alloc-Nα-Fmoc-lysine

Anna Crivici Guelph-Waterloo Centre for Graduate Work in Chemistry, Department of Chemistry, University of Waterloo, Waterloo, Ontario, Canada, N2L 3G1

Gilles Lajoie Guelph-Waterloo Centre for Graduate Work in Chemistry, Department of Chemistry, University of Waterloo, Waterloo, Ontario, Canada, N2L 3G1

Abstract

This report describes a convenient procedure for a 100 g scale preparation of Fmoc-Lys(Alloc) in 85% yield. This method can be easily adapted to a near one-pot procedure with slightly reduced yields, without requiring the isolation of the intermediate Lys(Alloc).

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A Procedure for the Large Scale Preparation of Nε-Alloc-lysine and Nε-Alloc-Nα-Fmoc-lysine

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A Procedure for the Large Scale Preparation of Nε-Alloc-lysine and Nε-Alloc-Nα-Fmoc-lysine

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