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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 14
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Original Articles

A Novel Perfluoroalkylation of Pyrroles with Perfluoroalkanesulfonyl chloride Catalyzed by a Ruthenium(II) Phosphine Complex

Nobumasa Kamigata Department of Chemistry, Faculty of Science, Tokyo Metropolitan University, Minami-ohsawa, Hachioji, Tokyo, 192-03, Japan
,
Takeshi Ohtsuka Department of Chemistry, Faculty of Science, Tokyo Metropolitan University, Minami-ohsawa, Hachioji, Tokyo, 192-03, Japan
,
Masato Yoshida Department of Chemistry, Faculty of Science, Tokyo Metropolitan University, Minami-ohsawa, Hachioji, Tokyo, 192-03, Japan
&
Toshio Shimizu Department of Chemistry, Faculty of Science, Tokyo Metropolitan University, Minami-ohsawa, Hachioji, Tokyo, 192-03, Japan
Pages 2049-2055 | Received 18 Jan 1994, Published online: 23 Sep 2006
 
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Abstract

Direct perfluoroalkylation of N-substituted pyrroles with tridecafluorohexanesulfonyl chloride catalyzed by a ruthenium(II) phosphine complex proceeds regioselectively in high yield.

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