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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 22
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Original Articles

Efficient One-Pot Procedures for the Preparation of Secondary Phosphines

L. Brandsma Department of Preparative, Organic Chemistry of the University, Padualaan 8, 3584 CH, Utrecht, The Netherlands
,
N. K. Gusarova Institute of Organic Chemistry of the Russian Academy of Sciences, Siberian Branch, Favorsky Street 1, 664033, Irkutsk, Russia
,
A. V. Gusarov Institute of Organic Chemistry of the Russian Academy of Sciences, Siberian Branch, Favorsky Street 1, 664033, Irkutsk, Russia
,
H. D. Verkruijsse Department of Preparative, Organic Chemistry of the University, Padualaan 8, 3584 CH, Utrecht, The Netherlands
&
B. A. Trofimov Institute of Organic Chemistry of the Russian Academy of Sciences, Siberian Branch, Favorsky Street 1, 664033, Irkutsk, Russia
Pages 3219-3223 | Received 12 May 1994, Published online: 23 Sep 2006
 
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Abstract

Secondary phosphines R2PH or RR'PH (R and R' = alkyl, cycloalkyl) have been obtained in good yields by preparing lithium phosphide from lithium, red phosphorus and t-butylalcohol in liquid ammonia and subsequent alkylation in the presence of alkali amide, prepared in the same flask.

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