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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 22
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Original Articles

Synthesis of Vinyl Sulfones from Aryl Methyl Ketones Under Sonochemical Conditions and Formation of Allyl Sulfones

H. El Fakih Laboratoire de Chimie Organique, Institut des Sciences Pharmaceutiques et Biologiques, Université Claude Bernard, 8 Avenue Rockefeller, 69373, Lyon Cedex 08, France
,
F. Pautet Laboratoire de Chimie Organique, Institut des Sciences Pharmaceutiques et Biologiques, Université Claude Bernard, 8 Avenue Rockefeller, 69373, Lyon Cedex 08, France
,
D. Peters Laboratoire de Chimie Organique, Institut des Sciences Pharmaceutiques et Biologiques, Université Claude Bernard, 8 Avenue Rockefeller, 69373, Lyon Cedex 08, France
,
H. Fillion Laboratoire de Chimie Organique, Institut des Sciences Pharmaceutiques et Biologiques, Université Claude Bernard, 8 Avenue Rockefeller, 69373, Lyon Cedex 08, France
&
J. L. Luche Laboratoire AMPERES, Université Paul Sabatier, 118 Route de Narbonne, 31062, Toulouse Cedex, France
Pages 3225-3233 | Received 07 Feb 1994, Published online: 23 Sep 2006
 
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Abstract

An efficient synthesis of vinyl sulfones 3a-o from aryl methyl ketones 2 bearing an electron withdrawing group and the phosphonic ester 1 under sonochemical conditions is reported. These compounds are generally obtained as an E/Z mixture. Formation of the allyl sulfones 4 is also observed.

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