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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 22
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Original Articles

Studies on the Preparation of Isocarbacyclin Intermediates. Part II

Masahiro Koga Iwakuni Pharmaceutical Factory, Chemicals Manufacturing Plant. Teijin Ltd., 2-1 Hinode-cho, Iwakuni, Yamaguchi, 740, Japan
,
Haruo Kageyama Iwakuni Pharmaceutical Factory, Chemicals Manufacturing Plant. Teijin Ltd., 2-1 Hinode-cho, Iwakuni, Yamaguchi, 740, Japan
,
Toshio Tanaka Iwakuni Pharmaceutical Factory, Chemicals Manufacturing Plant. Teijin Ltd., 2-1 Hinode-cho, Iwakuni, Yamaguchi, 740, Japan
&
Takao Fujii Iwakuni Pharmaceutical Factory, Chemicals Manufacturing Plant. Teijin Ltd., 2-1 Hinode-cho, Iwakuni, Yamaguchi, 740, Japan
Pages 3321-3329 | Received 04 Apr 1994, Published online: 23 Sep 2006
 
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Abstract

2,2,2-Trifluoroethanol was found to be an effective proton source for the reductive cyclization reaction of γ-ethynyl aldehyde 3 with lithium naphthalene providing the cyclized product 4, which is a useful isocarbacyclin synthon.

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