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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 17
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Original Articles

A Convenient Synthesis of 7,9,9-Trimethyl-1-oxaspiro[4,5]-6-decen-2-one

Drury Caine Department of Chemistry, University of Alabama, Tuscaloosa, AL, 35487, USA
&
Chia-Rong Lin Department of Chemistry, University of Alabama, Tuscaloosa, AL, 35487, USA
Pages 2473-2476 | Received 14 Mar 1994, Published online: 16 Feb 2007
 
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Abstract

The allylic lactone 1 was prepared from the reaction of lithium 3-lithiopropanoate (5) with isophorone (3) followed by mild acid treatment of the hydroxy acid adduct.

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