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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 17
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Original Articles

A Convenient Synthesis of Methyl (Z)-1-Carbamoyl-2-ethenylcyclopropanecarboxylate and (Z)-1-Carbamoyl-2-ethenylcyclopropanecarboxylic Acid

Michelle Galgoci Pharmaceuticals Process Research and Analytical Sciences, Core R&D, The Dow Chemical Company, Midland, MI, 48674
,
Janel E. Davidson Pharmaceuticals Process Research and Analytical Sciences, Core R&D, The Dow Chemical Company, Midland, MI, 48674
,
Clinton K. Harrington Pharmaceuticals Process Research and Analytical Sciences, Core R&D, The Dow Chemical Company, Midland, MI, 48674
,
Dennis L. Hasha Pharmaceuticals Process Research and Analytical Sciences, Core R&D, The Dow Chemical Company, Midland, MI, 48674
&
Christian T. Goralski Pharmaceuticals Process Research and Analytical Sciences, Core R&D, The Dow Chemical Company, Midland, MI, 48674
Pages 2477-2483 | Received 22 Feb 1994, Published online: 16 Feb 2007
 
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Abstract

A simple method for the preparation of the title compounds via the reaction of dimethyl 2-ethenylcyclopropane-1,1-dicarboxylate with 6M ammonia in methanol is described.

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