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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 4
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Original Articles

Synthesis and Structural Study of (+)-5-Acetyl-6-methyl-5p-tolylsulfinyl-3a,4,5,6-tetrahydro (3H)-Benzofuran-2-one

Christian Alexandre Laboratoire de Synthèse Organique, associé au CNRS, URA 482 Faculté des Sciences, Avenue O. Messiaen, BP 535, F-72017, Le Mans
,
Omer Belkadi Laboratoire de Synthèse Organique, associé au CNRS, URA 482 Faculté des Sciences, Avenue O. Messiaen, BP 535, F-72017, Le Mans
&
Francis Rouessac Laboratoire de Synthèse Organique, associé au CNRS, URA 482 Faculté des Sciences, Avenue O. Messiaen, BP 535, F-72017, Le Mans
Pages 447-452 | Published online: 04 Jan 2007
 
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Abstract

an efficient synthesis of the title compound has been developed from 3-phenyl sulfonylpropanoic acid via the butenolide 2. The key synthetic step is a Diels-Alder reaction. A mechanism is suggested.

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