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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 8
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Original Articles

A Convenient and Efficient Process to 5-(2-Di-n-Propylaminoethyl)-6-hydroxyindole

Christos G. Gourdoupis University of Patras, School of Health Sciences, Department of Pharmacy, Rion, Patras, 261 10, Hellas
,
Heleni K. Kotzamani University of Patras, School of Health Sciences, Department of Pharmacy, Rion, Patras, 261 10, Hellas
&
Ionnis K. Stamos The National Hellenic Research Foundation, Institute of Organic and Pharmaceutical Chemistry and the Center for Molecular Analysis, 48 V. Konstantinou Ave., Athens, 116 35, Hellas; University of Patras, Department of Pharmacy, Rion, Patras, 261 10, Hellas
Pages 1129-1136 | Received 30 Sep 1993, Published online: 23 Sep 2006
 
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Abstract

An intermolecular trapping of the Pummerer intermediate, generated from 9 with TFAA, by 4 at position 5 under mild Lewis acid conditions gave 5. Sequential treatment of 5 with Ra-Ni, LiAlH4 and again Ra-Ni, afforded 8 in high overall yield.

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