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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 1
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Original Articles

A Convenient Access to Dihydroxybenzenethiols via Reduction of Iso-Thiouronium Salts with Sodium Borohydride

D. Mascagna Department of Organic and Biological Chemistry, University of Naples, Via Mezzocannone 16, I-80134, Naples, Italy
,
M. d'Ischia Department of Organic and Biological Chemistry, University of Naples, Via Mezzocannone 16, I-80134, Naples, Italy
,
C. Costantini Department of Organic and Biological Chemistry, University of Naples, Via Mezzocannone 16, I-80134, Naples, Italy
&
G. Prota Department of Organic and Biological Chemistry, University of Naples, Via Mezzocannone 16, I-80134, Naples, Italy
Pages 35-42 | Received 03 Jun 1993, Published online: 23 Sep 2006
 
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Abstract

An improved procedure for the preparation of unstable dihydroxybenzenethiols in high yields is reported, involving mild reduction of the corresponding iso-thiouronium salts with sodium borohydride.

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