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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 1
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Original Articles

Selective Mono- and Bis-Oxidation of 2,6-bis(Hydroxy-methyl) phenols with Active Manganese Dioxide

Ru-Gang Xie Department of Chemistry, Sichuan University, Chengdu, 610064, P. R. China
,
Zhu-Jun Zhang Department of Chemistry, Sichuan University, Chengdu, 610064, P. R. China
,
Jia-Ming Yan Department of Chemistry, Sichuan University, Chengdu, 610064, P. R. China
&
De-Qi Yuan Department of Chemistry, Sichuan University, Chengdu, 610064, P. R. China
Pages 53-58 | Received 24 Jun 1993, Published online: 23 Sep 2006
 
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Abstract

Selective mono- and bis-oxidations of 2,6-bis(hydroxy-methyl) phenols with active Mn 2 were realized, giving 2-hydroxy-3-hydroxymethyl benzaldehydes and 2-hydroxyisophthalaldehydes in good yields. The influence of oxidant activity, reaction solvent and temperature on the selectivity were investigated, and favorable conditions developed.

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