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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 7
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Original Articles

An Improved Procedure for the Preparation of 4,5-Dinitrochrysazin

Pages 931-937 | Received 02 Sep 1993, Published online: 23 Sep 2006
 

Abstract

Pure 4,5-dinitrochrysazin was prepared by selective nitration of chrysazin, followed by solvent extraction of impurities. This method is suitable for scaling without need of chromatography, and represents a significant improvement over literature methods.

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