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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 2
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Original Articles

Titanium Mediated Cyclization of N-Substituted Di(β-Carbethoxyethyl)amines: Preparation of 1-Substituted-3-carbethoxy-4-piperidones

M. N. Deshmukh Indian Institute of Chemical Technology, Hyderabad, 500-007, India
,
U. Sampath Kumar Indian Institute of Chemical Technology, Hyderabad, 500-007, India
&
A. V. Rama Rao Indian Institute of Chemical Technology, Hyderabad, 500-007, India
Pages 177-182 | Received 23 May 1994, Published online: 23 Sep 2006
 
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Abstract

Dieckmann cyclisation of N-substituted di(β-carbethoxy-ethyl)amines with titanium tetrachloride in DCM in the presence of triethylamine leads to the formation of 3-carbethoxy-4-piperidones.

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