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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 3
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Original Articles

Chemoselective Removal of Allylic Formyloxy Group Using Sml2

K. Shibuya Tokyo Research Laboratories, Kowa Co., Ltd., 2-17-43 Noguchi-cho, Higashimurayama, Tokyo, 189, Japan
&
M. Shiratsuchi Tokyo Research Laboratories, Kowa Co., Ltd., 2-17-43 Noguchi-cho, Higashimurayama, Tokyo, 189, Japan
Pages 431-449 | Received 22 Jun 1994, Published online: 23 Sep 2006
 
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Abstract

A variety of allylic formates are chemoselectively transformed into the corresponding olefins in excellent yields on treatment with Sml2 in THF-HMPA-H2O (20:5:1), even though allylic acetate and allylic ether groups are present in the same molecule.

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