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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 4
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Original Articles

Synthesis of 3,5-Disubstituted Butenolides. A Short Preparation of Volatile Streptomyces Lactones

T. Howard Black Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920
,
Gary A. Brown Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920
,
Douglas C. Smith Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920
&
Sean M. Martinie Department of Chemistry, Eastern Illinois University, Charleston, IL, 61920
Pages 479-483 | Received 31 Jul 1994, Published online: 23 Sep 2006
 
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Abstract

α-Chloro carboxylic acid dianions condense with propanal to form β-lactones which, upon treatment with magnesium bromide, form 3,5-disubstituted butenolides.

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