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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 24
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Original Articles

Convenient Synthesis of Monoprotected 1,2-Diols

László Poppe Central Research Institute for Chemistry, Hungarian Academy of Sciences, H-1526, Budapest, P.O. Box 17, Hungary
,
Katalin Recseg Cereol Research & Development Centre, H-1095, Budapest, Kvassay J. út 1, Hungary
&
Lajos Novák Institute for Organic Chemistry, Technical University of Budapest, H-1111, Budapest, Gellért tér 4, Hungary
Pages 3993-4000 | Received 02 May 1995, Published online: 23 Sep 2006
 
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Abstract

Reaction of the protected glycidol derivatives (1A-C) with a wide variety of Grignard reagents (2a-h) in the presence of catalytic amount of CuCN provided the corresponding monoprotected diol derivatives (3) in a highly regioselective manner.

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