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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 17
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Original Articles

Preparation of Unsaturated Nitriles by the Modification of Mitsunobu-Wilk Procedure II Carbon Elongation of β-Acetylenic Alcohols

Mohammed C. Aesa Central Research Institute for Chemistry, Hugarian Academy of Sciences, P. O. Box 17, H-1525
,
Gábor Baán Central Research Institute for Chemistry, Hugarian Academy of Sciences, P. O. Box 17, H-1525
,
Lajos Novák Institute for Organic Chemistry, Technical University, 1111, Budapest, Gellért tér 4, Hungary
&
Csaba Szántay Central Research Institute for Chemistry, Hugarian Academy of Sciences, P. O. Box 17, H-1525; Institute for Organic Chemistry, Technical University, 1111, Budapest, Gellért tér 4, Hungary
Pages 2575-2578 | Received 30 Dec 1994, Published online: 23 Sep 2006
 
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Abstract

An efficient one-step procedure for the converison of β-acetylenic alcohols into the corresponding nitriles using triphenylphosphine (PPh3)-diethyl azodicarboxylate (DEAD) in the presence of acetone cyanohydrin is described.

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