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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 17
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Original Articles

Preparation and Use of Lithium Tritide and Lithium Trimethoxyborotritide

E. M. Zippi National Tritium Labelling Facility, Structural Biology Division, Lawrence Berkeley Laboratory, Berkeley, CA, 94720, U.S.A.; Department of Chemistry and Physics, Louisiana State University, Shreveport, LA, 71115, U.S.A.
,
H. Andres Sandoz Pharma Ltd, Chemical Research and Development, Basle, CH-4002, Switzerland
,
H. Morimoto National Tritium Labelling Facility, Structural Biology Division, Lawrence Berkeley Laboratory, Berkeley, CA, 94720, U.S.A.
&
P. G. Williams National Tritium Labelling Facility, Structural Biology Division, Lawrence Berkeley Laboratory, Berkeley, CA, 94720, U.S.A.
Pages 2685-2693 | Received 01 Dec 1994, Published online: 23 Sep 2006
 
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Abstract

Two new tritide reducing agents, Li3H and Li(CH3O)3B3H, have been prepared at the carrier-free level and used to reduce 2-naphthaldehyde to tritiated β-naphthalene methanol, to produce C3H3OR, and to synthesize a methyl-tritiated secondary amine.

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