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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 8
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Original Articles

A Convenient Synthesis of N-Methoxy-N-Methylamides from Carboxylic Acids

Mukund P. Sibi Department of Chemistry, North Dakota State University Fargo, ND, 58105
,
Chad C. Stessman Department of Chemistry, North Dakota State University Fargo, ND, 58105
,
Jeffrey A. Schultz Department of Chemistry, North Dakota State University Fargo, ND, 58105
,
James W. Christensen Department of Chemistry, North Dakota State University Fargo, ND, 58105
,
Jianliang Lu Department of Chemistry, North Dakota State University Fargo, ND, 58105
&
Mali Marvin Department of Chemistry, North Dakota State University Fargo, ND, 58105
Pages 1255-1264 | Received 11 Oct 1994, Published online: 23 Sep 2006
 
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Abstract

Carboxylic acids can be converted to their corresponding N-methoxy-N-methylamides in high yields using 2-chloro-1-methylpyridinium iodide as the coupling agent. The reaction proceeds without racemization when chiral carboxylic acids are used as the starting material.

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