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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 16
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Original Articles

A Convenient Synthetic Method for Alpha-Alkylation of Steroidal 17-Ketone: Preparation of 16β(THPO-Heptyl)-Estradiol

Martin R. Tremblay Medicinal Chemistry Division Laboratory of Molecular Endocrinology, CHUL Research Center and Laval University, Quebec, QcG1V4G2
,
Serge Auger Medicinal Chemistry Division Laboratory of Molecular Endocrinology, CHUL Research Center and Laval University, Quebec, QcG1V4G2
&
Donald Poirier Medicinal Chemistry Division Laboratory of Molecular Endocrinology, CHUL Research Center and Laval University, Quebec, QcG1V4G2
Pages 2483-2495 | Received 03 Jan 1995, Published online: 04 Jan 2007
 
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Abstract

A sequence of three key-steps (activation of steroidal 17-ketone, alkylation and decarboxyalkoxylation) provided an interesting synthetic device to obtain, after reduction, 16β-(THPO-heptyl)-estradiol.

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