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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 22
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Original Articles

A Convenient Method for the Preparation of N-Aryl and N-Alkyl-O-Methyl Hydroxylamines

Paulo F. Santos Secção de Química Org[acaron]nica Aplicada, Departamento de Química, and SINTOR-UNINOVA, campus FCT-UNL, Quinta da Torre, 2825, Monte da Caparica, Portugal
,
Ana M. Lobo Secção de Química Org[acaron]nica Aplicada, Departamento de Química, and SINTOR-UNINOVA, campus FCT-UNL, Quinta da Torre, 2825, Monte da Caparica, Portugal
&
Sundaresan Prabhakar Secção de Química Org[acaron]nica Aplicada, Departamento de Química, and SINTOR-UNINOVA, campus FCT-UNL, Quinta da Torre, 2825, Monte da Caparica, Portugal
Pages 3509-3518 | Received 23 Mar 1995, Published online: 23 Sep 2006
 
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Abstract

Trifluoroaceto or p-nitrobenzo-N-substituted hydroxamic acids are smoothly methylated with diazomethane and the products cleanly cleaved by hydrazine to provide the title compounds.

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