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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 22
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Original Articles

Improved Synthesis of Methyl 4,6-O-Benzylidene-3-cyano-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside and Methyl 4,6-O-Benzylidene-2,3-dideoxy-3-C-formyl-α-D-erythro-hex-2-enopyranoside

Rolando A. Spanevello Institute de Química Orgánica de Síntesis CONICET - Universidad Nacional de Rosario, Facultad de Ciencias Bioquímicas y Farmacéuticas, Casilla de Correo 991, 2000, Rosario, Argentina
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Silvina C. Pellegrinet Institute de Química Orgánica de Síntesis CONICET - Universidad Nacional de Rosario, Facultad de Ciencias Bioquímicas y Farmacéuticas, Casilla de Correo 991, 2000, Rosario, Argentina
Pages 3663-3670 | Received 13 Apr 1995, Published online: 23 Sep 2006
 
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Abstract

Simple and efficient route to the title compounds by using diethyl aluminium cyanide in benzene for the epoxide ring opening and the electrophilic assistance of LiCIO4 during the isomerization-elimination process.

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