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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 11
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Original Articles

Hypervalent Iodine in Synthesis

X V II. Action of Phenyliodine (III) Dicarboxylates on Diaryl Ditellurides: A New and Facile Method for the Preparation of Arenetellurinic Mixed Anhydrides and Arenetellurinic Anhydrides

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Pages 1605-1616 | Received 21 Jun 1994, Published online: 23 Sep 2006
 

Abstract

A new and facile method for the preparation of arenetellurinic mixed anhydrides is described from diaryl ditellurides and phenyliodine (III) dicarboxylates. Hydrolysis of the arenetellurinic mixed anhydrides gives arenetellurinic anhydrides and a one - pot procedure involving the reaction of diaryl ditellurides with phenyliodine (III) dicarboxylates in a two - phase system of methylene chloride and aqueous solution of sodium hydroxide for the preparation of arenetellurinic anhydrides is provided.

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