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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 11
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Original Articles

Hypervalent Iodine in Synthesis

X IX. Oxidation of Aldehyde Hydrazones with Phenyliodine Diacetate: A New Method for the Generation of Nitrilimines

Da Wei Chen Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
&
Zhen Chu Chen Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
Pages 1617-1626 | Received 09 Sep 1994, Published online: 23 Sep 2006
 
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Abstract

Oxidation of aldehyde hydrazones with phenyliodine diacetate (PID) generated nitrilimines which were trapped by acrylonitrile to give 1, 3-disubstituted 2-pyrazoline-5-carbonitriles in good yields.

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