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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 11
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Original Articles

Hydrotalcite-Catalyzed Alkylation of 2,4-Pentanedione

C. Cativiela Departamento de Química Orgánica, Instituto de Ciencia de Materiales de Aragón, Universidad de Zaragoza-C.S.I.C., 50009, Zaragoza, España
,
F. Figueras Institut de Recherches sur la Catalyse. C.N.R.S. 2, Avenue Albert Einstein, 69626, Villeurbanne Cedex, France
,
J. I. García Departamento de Química Orgánica, Instituto de Ciencia de Materiales de Aragón, Universidad de Zaragoza-C.S.I.C., 50009, Zaragoza, España
,
J. A. Mayoral Departamento de Química Orgánica, Instituto de Ciencia de Materiales de Aragón, Universidad de Zaragoza-C.S.I.C., 50009, Zaragoza, España
&
M. M. Zurbano Departamento de Química Orgánica, Instituto de Ciencia de Materiales de Aragón, Universidad de Zaragoza-C.S.I.C., 50009, Zaragoza, España
Pages 1745-1750 | Received 17 Sep 1994, Published online: 23 Sep 2006
 
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Abstract

A synthetic anionic clay, hydrotalcite (Mg/Al = 2.8), calcined under dry air at 450 [ddot]C, has proved to be an efficient catalyst for the selective C-monoalkylation of 2,4-pentanedione with reactive alkylating reagents.

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