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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 11
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Original Articles

A Facile Synthesis of 3,4-Dialkoxythiophenes

M. Coffey Department of Chemistry, Wright State University, Dayton, OH, 45435
,
B. R. McKellar Department of Chemistry, Wright State University, Dayton, OH, 45435
,
B. A. Reinhardt Polymer Branch, Materials Directorate, Wright Laboratory, Wright-Patterson AFB, OH, 45433-6533
,
T. Nijakowski Department of Chemistry, Wright State University, Dayton, OH, 45435
&
W. A. Feld Department of Chemistry, Wright State University, Dayton, OH, 45435
Pages 2205-2212 | Received 11 Nov 1995, Published online: 21 Aug 2006
 
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Abstract

Dialkylation of diethyl 3,4-dihydroxythiophenedicarboxylate followed by ester hydrolysis and acid decarboxylation provides a general route to 3,4-dialkoxythiophenes.

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