Synthesis of Terminal Perfluoroalkyl Enol Ethers and Epoxy Ethers

Jean-Pierre Bégué BioCIS-CNRS, Centre d'Etudes Pharmaceutiques, Rue J.B. Clëment, F-92296 Châtemay-Malabry, France

Danièle Bonnet-Delpon BioCIS-CNRS, Centre d'Etudes Pharmaceutiques, Rue J.B. Clëment, F-92296 Châtemay-Malabry, France

Andrei Institute of Bioorganic Chemistry and Petrochemistry, Ukrainian Academy of Sciences, MurmanskayaSt. 1, 253160, Kiev, Ukraine

Abstract

A practical method for the multigram-scale preparation in good yields of terminal perfluoroalkyl enol ethers, using Wittig olefination of perfluoroalkyl ethers, is reported. The corresponding epoxy ethers are available via their m-CPBA epoxidation in good yields.

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Synthesis of Terminal Perfluoroalkyl Enol Ethers and Epoxy Ethers

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Synthesis of Terminal Perfluoroalkyl Enol Ethers and Epoxy Ethers

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