Advanced search
Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 21
Submit an article Journal homepage
186
Views
20
CrossRef citations to date
0
Altmetric
Original Articles

A “One-Pot” Phase Transfer Alkylation/Hydrolysis of o-Nitrotrifluoroacetanilides. A Convenient Route to N-ALKYL o-Phenylenediamines

Samuel A. Brown Department of Chemistry, Vanderbilt University, Box 1822, Station B;, Nashville, TN, 37235
&
Carmelo J. Rizzo Department of Chemistry, Vanderbilt University, Box 1822, Station B;, Nashville, TN, 37235
Pages 4065-4080 | Received 24 May 1996, Published online: 23 Aug 2006
 
Sample our Physical Sciences journals, sign in here to start your FREE access for 14 days

Abstract

A variety of o-nitrotrifluoroacetanilides undergo a one-pot alkylation/hydrolysis to give N-alkyl o-nitroanilines in 40–94% yield. Dimethylsulfate, benzyl bromide and 1-bromo-propane were used as the electrophiles.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Order Reprints Request Corporate Permissions

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

Request Academic Permissions

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.

Related research

People also read lists articles that other readers of this article have read.

Recommended articles lists articles that we recommend and is powered by our AI driven recommendation engine.

Cited by lists all citing articles based on Crossref citations.
Articles with the Crossref icon will open in a new tab.