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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 1
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Original Articles

Sand Catalyzed Oxidative Cleavage of Double Bonds

Bingnan Huang Department of Chemistry, Lamar University, Beaumont, TX, 77710
,
John T. Gupton Department of Chemistry, Lamar University, Beaumont, TX, 77710
,
Keith C. Hansen Department of Chemistry, Lamar University, Beaumont, TX, 77710
&
John P. Idoux Department of Chemistry, Lamar University, Beaumont, TX, 77710
Pages 165-178 | Received 15 May 1995, Published online: 21 Aug 2006
 
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Abstract

The discovery of a catalytic effect of sand on the activity of KMnO4/NaIO4 or KMnO4/NaClO oxidant system provides a convenient method for double bond cleavage under mild conditions. An oxidative rearrangement of α-bromostyrene to 2-bromoacetophenone was also observed.

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