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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 15
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Original Articles

Preparation of Dialkyl Disulfides via Reduction of Alkylthiocyanates with TiCl4/Sm System

Hongyun Guo Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
,
Zhuangping Zhan Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
&
Yongmin Zhang Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
Pages 2721-2724 | Received 10 Jan 1997, Published online: 22 Aug 2006
 
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Abstract

Dialkyl disulfides can be readily prepared in moderate to good yields via reduction of alkylthiocyanates with TiCl4/Sm system in THF at 0°C.

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