Improved Synthesis of (4S)-4-[(1S,2R)-1,2-Epoxybut-3-enyl]-2-phenyl-2-oxazoline, a Key Intermediate for Sphingolipids¹

Teiichi Murakami National Institute of Materials and Chemical Research, 1-1 Higashi, Tsukuba, Ibaraki, 305, Japan

Toshimi Shimizu National Institute of Materials and Chemical Research, 1-1 Higashi, Tsukuba, Ibaraki, 305, Japan

Abstract

Abstract: The title compound has been conveniently synthesized from N-benzoyl-D-glucosamine by a novel route using oxidative bromination of benzylidene acetal as a key step.

Notes

Synthetic studies on sphingolipids. Part 4. For Part 3, see ref. 2.

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Improved Synthesis of (4S)-4-[(1S,2R)-1,2-Epoxybut-3-enyl]-2-phenyl-2-oxazoline, a Key Intermediate for Sphingolipids¹

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Improved Synthesis of (4S)-4-[(1S,2R)-1,2-Epoxybut-3-enyl]-2-phenyl-2-oxazoline, a Key Intermediate for Sphingolipids1

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Improved Synthesis of (4S)-4-[(1S,2R)-1,2-Epoxybut-3-enyl]-2-phenyl-2-oxazoline, a Key Intermediate for Sphingolipids¹