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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 11
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Original Articles

A Facile Regioselective 1,6-O-Diacetylation Method of Methyl-Glycopyranosides and Their Dimethyl Phosphonates

Guang-tao Zhang National Laboratory of Bio-organic and Natural Products Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, 200032, China; Department of Chemical Physics, the University of Science and Technology of China, Hefei, 230026, China
,
Zhong-wu Guo National Laboratory of Bio-organic and Natural Products Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, 200032, China
&
Yong-zheng Hui National Laboratory of Bio-organic and Natural Products Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, 200032, China
Pages 1907-1917 | Received 28 Oct 1996, Published online: 22 Aug 2006
 
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Abstract

A general method of 1,6-di-O-acetylation of methyl-ä/β-glycopyranosides and a strategy to synthesize protected dimethyl (2,3,4-tri-O-benzyl-α-D-glycosyl) phosphonate having a free OH at C-6 are reported.

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