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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 18
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Original Articles

A New Application of Dimethyl Trithiocarbonate. Methylthiothiocarbonylation of 2,4-Pentanedione and Some β-Oxoesters

A. Oliva Instituto de Química, Universidad Católica de Valparaíso, casilla 4059, Valparaíso, Chile
,
A. Molinari Instituto de Química, Universidad Católica de Valparaíso, casilla 4059, Valparaíso, Chile
&
L. Sánchez Instituto de Química, Universidad Católica de Valparaíso, casilla 4059, Valparaíso, Chile
Pages 3381-3386 | Received 30 Mar 1998, Published online: 22 Aug 2006
 
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Abstract

2,4-Pentanedione, ethyl acetoacetate, benzoyl acetate and diethyl malonate 1a-d react with sodium acetate and dimethyl trithiocarbonate in dimethylformamide to afford methyl-β,β′-dicarbonyldithiocarboxylate derivatives 2a-d in moderate yield.

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