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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 18
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Original Articles

Synthesis of Resorcinols via a Michael Addition-Dieckman Cyclization Sequence of Dimethyl 1,3-Acetonedicarboxylate Anion with Alkyl Alkynoates

A. Covarrubias-Zúñiga Instituto de Química, Universidad Nacional Autónoma de México, Circuito Exterior, Ciudad Universitaria, Coyoacán, 04510, México
,
L. A. Maldonado Instituto de Química, Universidad Nacional Autónoma de México, Circuito Exterior, Ciudad Universitaria, Coyoacán, 04510, México
,
E. Ríos-Barrios Instituto de Química, Universidad Nacional Autónoma de México, Circuito Exterior, Ciudad Universitaria, Coyoacán, 04510, México
&
A. González-Lucas Instituto de Química, Universidad Nacional Autónoma de México, Circuito Exterior, Ciudad Universitaria, Coyoacán, 04510, México
Pages 3461-3469 | Received 06 Apr 1998, Published online: 22 Aug 2006
 
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Abstract

The reaction of dimethyl 1,3-acetonedicarboxylate anion 1 with a number of alkyl alkynoates gives unsymmetrical (from alkynoates 2a-g) or symmetrical (from alkynoates 2h-i) resorcinols, in a one pot synthesis.

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