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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 18
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Original Articles

Synthesis of New Macrobicyclic Hexaamide Ligands

Z. Mo Department of Chemistry, Northwest Normal University, Lanzhou, 730070, China
,
W. Yang Department of Chemistry, Northwest Normal University, Lanzhou, 730070, China
,
J. Gao Department of Chemistry, Northwest Normal University, Lanzhou, 730070, China
,
H. Chen Department of Chemistry, Northwest Normal University, Lanzhou, 730070, China
,
Q. Gong Department of Chemistry, Northwest Normal University, Lanzhou, 730070, China
,
J. Hou Department of Chemistry, Northwest Normal University, Lanzhou, 730070, China
&
J. Kang Department of Chemistry, Northwest Normal University, Lanzhou, 730070, China
 show all
Pages 3503-3508 | Received 07 Apr 1998, Published online: 22 Aug 2006
 
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Abstract

A new two-step synthesis method of macrobicyclic hexaamide ligands LH6 (I and II) with double condensation of triethyl nitrilotriacetate and 1,4(1,2)-diaminobenzene was developed. The cyclization does not require high dilution and template techniques. Two new hexaamide ligands were prepared in good yields according to the proposed method.

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