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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 14
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Original Articles

A Convenient Route to Condensed-Ring Aromatic Acetylenes

Geoffrey T. Crisp Department of Chemistry, The University of Adelaide, Adelaide, S. A. Australia, 5005
&
Yu-Lin Jiang Department of Chemistry, The University of Adelaide, Adelaide, S. A. Australia, 5005
Pages 2571-2576 | Received 21 Nov 1997, Published online: 20 Aug 2006
 
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Abstract

Palladium catalysed coupling of aryl halides with 3-methylbut-1-yn-3-ol and a subsequent base-induced retro-Favorsky reaction gave the corresponding ethynyl aromatics in good to excellent yields.

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