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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 15
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Original Articles

A New Method for Synthesis of Functionalized Organozinc-Copper(I) Reagents and Their 1,4-Addition Reaction with Enones

Yulai Hu State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P.R. China
,
Jianhua Yu State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P.R. China
,
Shiyan Yang State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P.R. China
,
Jin-Xian Wang Department of Chemistry, Northwest Normal University, Lanzhou, 730070, P.R. China
&
Yuanqi Yin State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P.R. China
Pages 2793-2800 | Received 27 Jan 1998, Published online: 20 Aug 2006
 
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Abstract

The transmetalation of functionalized organozinc iodides with Cu(OAc)2 in THF provides a new convenient method for the preparation of functionalized organozinc-copper(I) reagents FG-RCu(OAc)ZnI which ultimately undergo 1,4-addition reaction with enones to give the products in good to excellent yields.

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