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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 16
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Original Articles

A Simple and Efficient Procedure for Oxidation of Sulfides to Sulfoxides on Hydrated Silica Gel with Ceric Ammonium Nitrate (Can) In Methylene Chloride

Mohammed Hashmat Ali Department of Chemistry, Southeast Missouri State University, Cape Girardeau, Missouri, 63701, U. S. A.
,
Damon R. Leach Department of Chemistry, Southeast Missouri State University, Cape Girardeau, Missouri, 63701, U. S. A.
&
Chad E. Schmitz Department of Chemistry, Southeast Missouri State University, Cape Girardeau, Missouri, 63701, U. S. A.
Pages 2969-2981 | Received 05 Mar 1998, Published online: 23 Aug 2006
 
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Abstract

A simple, fast and efficient procedure for oxidation of sulfides to the corresponding sulfoxides with CAN mediated by hydrated silica gel in methylene chloride has been developed. To our knowledge, this is the first example of oxidation of sulfides with CAN in a non-aqueous media.

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