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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 16
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Original Articles

Oxone® Promoted Nef Reaction. Simple Conversion of Nitro Group Into Carbonyl

Paolo Ceccherelli† Istituto di Chimica Organica, Facoltà di Farmacia, Università degli Studi, Via del Liceo, 06123, Perugia, Italy
,
Massimo Curini Istituto di Chimica Organica, Facoltà di Farmacia, Università degli Studi, Via del Liceo, 06123, Perugia, Italy
,
Maria Carla Marcotullio Istituto di Chimica Organica, Facoltà di Farmacia, Università degli Studi, Via del Liceo, 06123, Perugia, Italy
,
Francesco Epifano Istituto di Chimica Organica, Facoltà di Farmacia, Università degli Studi, Via del Liceo, 06123, Perugia, Italy
&
Ornelio Rosati Istituto di Chimica Organica, Facoltà di Farmacia, Università degli Studi, Via del Liceo, 06123, Perugia, Italy
Pages 3057-3064 | Received 06 Mar 1998, Published online: 23 Aug 2006
 
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Abstract

A mild and convenient oxidative Nef reaction using Oxone® (potassium hydrogen persulfate) is described. Following our procedure primary and secondary nitroalkanes generate carboxylic acids and ketones, respectively, both in good yields.

†Deceased on January 1st 1998

Notes

†Deceased on January 1st 1998

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