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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 16
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Original Articles

Reaction of β-Oxodithioesters With Propargylamine: A Facile Entry to Novel 2-(Acylalkylidene)-5-(Methylene)Thiazolidines

M. Chandrasekharam Department of Chemistry, North-Eastern Hill University, Shillong, 793 003, Meghalaya, India
,
O. Mukherjee Singh Department of Chemistry, North-Eastern Hill University, Shillong, 793 003, Meghalaya, India; Department of Chemistry, Manipur University, Canchipur, Imphal, 795 003, Manipur, India
,
H. Ila Department of Chemistry, Indian Institute of Technology, Kanpur, 208 016, U.P., India
&
H. Junjappa Department of Chemistry, North-Eastern Hill University, Shillong, 793 003, Meghalaya, India
Pages 3073-3079 | Received 05 Mar 1998, Published online: 23 Aug 2006
 
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Abstract

Reaction of β-oxodithioesters derived from acyclic and cyclic ketones with propargylamine affords novel 2-(acylalkylidene)-5-(methylene)-thiazolidines in high yields by intramolecular nucleophilic attack of thiocarbonyl sulfur on the triple bond of the β-oxo-N-propargylthioamide intermediates.

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