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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 19
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Original Articles

A New and Facile Synthetic Route to 1-Alkyl-2-Oxopropylphosphonates : 1-Alkylation with Subsequent Ozonolysis of 2-Methyl Allylic Phosphonates

Jun MoGil Department of Chemistry, Korea Advanced Institute of Science and Technology, 373–1 Kusung-Dong, Yusung-Gu, Taejon, 305-701, Korea
,
Kwang YoungPark Department of Chemistry, Korea Advanced Institute of Science and Technology, 373–1 Kusung-Dong, Yusung-Gu, Taejon, 305-701, Korea
,
Jung HwanHah Department of Chemistry, Korea Advanced Institute of Science and Technology, 373–1 Kusung-Dong, Yusung-Gu, Taejon, 305-701, Korea
&
Dong YoungOh Department of Chemistry, Korea Advanced Institute of Science and Technology, 373–1 Kusung-Dong, Yusung-Gu, Taejon, 305-701, Korea
Pages 3601-3607 | Received 07 Apr 1998, Published online: 22 Aug 2006
 
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Abstract

Alkylation of the 2-methyl allylic phosphonates is performed by treatment with n-BuLi, followed by addition of alkyl halides. The 1-alkyl-2-oxopropylphosphonates are obtained by the ozonolysis of the corresponding allylic phosphonates.

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