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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 20
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Original Articles

Non Solvent Reaction: Ammonium Acetate Catalyzed Highly Convenient Preparation of Trans-Cinnamic Acids

H. M. SawpathKumar Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, INDIA
,
B. V. Subbareddy Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, INDIA
,
S. Anjaneyulu Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, INDIA
&
J. S. Yadav Organic Chemistry Division-I, Indian Institute of Chemical Technology, Hyderabad, 500 007, INDIA
Pages 3811-3815 | Received 27 Apr 1998, Published online: 23 Aug 2006
 
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Abstract

trans-Cinnamic acids were obtained in near quantitative yield when various aromatic aldehydes were heated with equimolar quantity of malonic acid in presence of ammonium acetate under solvent free conditions. Considerable enhancement in the rate of the reaction was observed when the decarboxylative condensation was carried out under microwave irradiation.

HCT Communication No. 3922

Notes

HCT Communication No. 3922

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