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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 21
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Original Articles

A General Synthesis of Functionalized Primary t-Alkylamines

Goerge T. Lee Process R&D, Chemical and Analytical Development, Novartis Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936, U.S.A.
,
Andrew Kucerovy Process R&D, Chemical and Analytical Development, Novartis Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936, U.S.A.
,
Kapa Prasad Process R&D, Chemical and Analytical Development, Novartis Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936, U.S.A.
,
Oljan Repic Process R&D, Chemical and Analytical Development, Novartis Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936, U.S.A.
&
Thomas J. Blacklock Process R&D, Chemical and Analytical Development, Novartis Pharmaceuticals Corporation, 59 Route 10, East Hanover, NJ, 07936, U.S.A.
Pages 4009-4018 | Received 14 May 1998, Published online: 16 Aug 2006
 
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Abstract

A simple and efficient γ-acetamidopropylation of different nucleophiles using oxazine 3 has been developed. Deacetylation of acetamides with titanium(IV) isopropoxide/diphenylsilane is also described.

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