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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 1
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Original Articles

A Convenient Synthesis of Cycloalkylphosphonates from (Phenylsulfonyl)methylphosphonate

Dae Young Kim Department of Chemistry, Soonchunhyang University, Asan, P. O. Box 97, Chungnam, 336-600, Korea
&
Ki Hyung Suh Department of Chemistry, Soonchunhyang University, Asan, P. O. Box 97, Chungnam, 336-600, Korea
Pages 83-91 | Received 04 Jun 1997, Published online: 20 Aug 2006
 
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Abstract

Cycloalkylphosphonate derivatives were synthesized in excellent overall yields, in two steps by the bis-alkylation of (phenylsulfonyl)methyl-phosphonate with ω-dibromoalkanes in the presence of a phase transfer catalyst followed by desulfonation.

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