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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 1
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Original Articles

Synthesis of Lactones via the Oxidation of α,ω-Diols with Sodium Bromite and Alumina Under Water Free Conditions

Masao Hirano Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, Japan
,
Shigetaka Yakabe Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, Japan
&
Takashi Morimoto Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, Japan
Pages 123-130 | Received 27 Jun 1997, Published online: 20 Aug 2006
 
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Abstract

Oxidation of α,ω-diols with sodium bromite can be readily performed in dichloromethane to afford lactones in fair good yield under mild and neutral conditions with the aid of chromatographic acidic alumina.

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