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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 3
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Original Articles

Dechlorination of Pentachlorophenol and 1,2,4-Trichlorobenzene Using NaBH4 and NaBH4/LiCl AT 125–315°C in Glyme Solvents

Cangming Yang Department of Chemistry University/Industry Chemical, Research Center Mississippi State University, Mississippi, 39762
&
Charles U. Pittman Jr. Department of Chemistry University/Industry Chemical, Research Center Mississippi State University, Mississippi, 39762
Pages 517-525 | Received 20 Jul 1997, Published online: 15 Aug 2006
 
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Abstract

Dechlorinations of pentachlorophenol and 1,2,4-trichlorobenzene were achieved using NaBH4 in tetraglyme at 290–315°C and by NaBH4/LiCl at 125–135°C in diglyme, triglyme or tetraglyme after premixing at room temperature.

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