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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 4
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Original Articles

Regioselective Aromatic Monobromination of Alkyl Phenyl Ethers with NaClO2, NaBr, Mn(acac)3, and Montmorillonite K10 in Dichloromethane

Masao Hirano Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, Japan
,
Shigetaka Yakabe Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, Japan
,
Hiroyuki Monobe Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, Japan
&
Takashi Morimoto Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, Japan
Pages 669-676 | Received 15 Aug 1997, Published online: 02 Sep 2006
 
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Abstract

Regioselective and high-yielding nuclear monobromination of aromatic ethers can be accomplished with a combination of NaClO2, NaBr, and Mn(acac)3 catalyst in dichloromethane under mild and neutral conditions with the aid of Montmorillonite K10.

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