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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 10
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Original Articles

Iodosobenzene Diacetate and Diphenyl Diselenide: An Electrophilic Selenenylating Agent of Double Bonds

Marco Tingoli* Istituto di Chimica Organica, Università di Perugia, 06100, Perugia, Italy
,
Marcello Tiecco Istituto di Chimica Organica, Università di Perugia, 06100, Perugia, Italy
,
Lorenzo Testaferri Istituto di Chimica Organica, Università di Perugia, 06100, Perugia, Italy
&
Andrea Temperini Istituto di Chimica Organica, Università di Perugia, 06100, Perugia, Italy
Pages 1769-1778 | Received 20 Oct 1997, Published online: 20 Aug 2006
 
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Abstract

Phenylseleno-acetoxylation, hydroxylation, etherification and lactonization products are obtained in good yields from the reaction of alkenes with diphenyl diselenide and iodosobenzene diacetate, in acetonitrile.

present address: Dipartimento di Scienza degli Alimenti, Università di Napoli “Federico II” Via Università, 100 - 80055-Portici, Napoli-Italy. e-mail [email protected].

Notes

present address: Dipartimento di Scienza degli Alimenti, Università di Napoli “Federico II” Via Università, 100 - 80055-Portici, Napoli-Italy. e-mail [email protected].

CH3CN gave better results in respect to CH2Cl2

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